The preparation and characterization of sulfamic acid-intercalated layered double hydroxide
作者：江玉, 谷曉昱, 張勝*, 唐武飛, 趙靜然
關鍵字：Layered double hydroxide; Intercalation; Composite materials; XPS; Flammability
論文來源：期刊
具體來源：Materials Letters
發表時間：2015年
NH2SO3-1 was intercalated into layered double hydroxide to prepare a novel sulfamic acid-intercalated MgAl-LDH (SA-LDH). Fourier transform infrared (FT-IR) analysis confirmed the presence of sulfamic acid in LDH. X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS) and transmission electron microscopy (TEM) were also used to characterize the structural morphology of SA-LDH, and the results revealed that the interlayer space of LDH had been enlarged from 0.76 to 0.91 nm and proved the formation ofhydrogen bonds between SA-LDH. The SA-LDH was introduced into ethylene vinyl acetate (EVA) copolymer via melt blending, and the cone calorimetry test results demonstrated that the presence of SA-LDH could significantly improve the flame retardancy of EVA composite.